博驰智能液质三重四极(TQ)质谱产品包括用于样品分析的液相色谱、三重四极杆质谱仪。
将每一种分析方法优化到实现分析物的色谱分离、高灵敏度检测和分析。安益谱液质联用控制软件帮助用户节约样品序列设置、提交、下发和运行时间，使用户能够快速运用。
LCMSMS TQ-9001产品特性
离子源
ESI/APCI快速切换、智能识别
即插即用、气电自动对接安装
90°直角喷雾、抗污染能力强.
质量分析器
串联金属四极杆设计，无限接近四极杆理论电场
前后预杆，有效平衡离子入射角度，消除边缘场效应.
碰撞反应池
180°碰撞反应池，去除中性粒子干扰
具有轴线加速电场，减小MRM通道间串扰
组合阵列式碰撞气体控制，保障碰撞反应的高效进行
强大的数据采集和分析软件 —— B&C ITECH Chemstation
中(英)文操作界面
集成仪器控制、调谐校准、数据采集、数据处理等功能
| 序号 | 名称/型号/规格 | 数量 | 单位 | 备注 |
| 一 | 标准配置 | |||
| 1 | 主机 | |||
| 1.1 | TQ-9001三重四极杆质谱仪 | 1 | 台 | 含ESI、APCI离子源，集成注射泵、切换阀，一体式差分涡轮分子泵400/300 L/s，前级机械泵40 m3/h |
| 1.2 | SPH1299 二元泵 | 1 | 台 | 二元超高压液相泵组，压力1300 bar，内置在线真空脱气机 |
| 1.3 | Alias 自动进样器 | 1 | 台 | 制冷型、标配2个48位样品瓶架 |
| 1.4 | T190柱温箱 | 1 | 台 | |
| 1.5 | 溶剂柜 | 1 | 台 | |
| 1.6 | 废液底座 | 1 | 台 | |
| 1.7 | SV40机械泵 | 1 | 台 | 内含预装泵油1瓶 |
| 2.1 | B&C ITECH Chemstation V1.0数据采集软件 | 1 | 套 | |
| 2.2 | B&C ITECH Chemstation数据处理软件 | 1 | 套 | |
| 2.3 | ||||
| 3 | 外设/附件 | |||
| 3.1 | 启动工具包： | 1 | 套 | 随机工具盒1套； 软件1个； 软件U盘1个； ESI 调谐液1瓶； 注射泵连接套装1套： 1ml 注射器、 鲁尔接头、PEEK管线、PEEK 接头； 安装搬运工具1套； 真空连接套件： 波纹管1根，KF40 卡箍2个，KF40 中心支架2个 备用密封圈1套： 离子源密封圈4个 QJET前密封圈1个 QJET后密封圈1个 反吹气密封圈1个； |
| 3.2 | 仪器说明书 | 1 | 份 | |
| 3.3 | 产品合格证、保修卡 | 1 | 套 | |
| 3.4 | ||||
| 选配品 | ||||
| 1.1 | 电脑 | 1 | 台 | |
| 1.2 | 打印机 | 1 | 台 | |
| 2 | ||||
| 2.1 | UPS稳压电源 | 1 | 台 | |
| 2.2 | 氮气发生器 | 1 | 台 | |
| 2.3 | ||||
| 4 | 备品/耗材 | |||
| 4.1 | 色谱柱 | 1 | 根 | |
| 4.2 | 样品瓶 | 1 | 套 | |
| 4.3 | 样品瓶盖 | 1 | 套 | |
B&C ITECH TQ9001 Triple Quad LC-MS/MS System
Instrument Specifications
| Instrument Specification-Mass spectrometer (Triple Quadruple) | |
| Mass range(m/z) | 5-2000 amu |
| Scan speed | >10,000 amu/sec |
| Mass Resolution | Unit Resolution FWHM，0.6-0.8 amu |
| Mass stability | ± 0.1Da in 24 hours |
| Sensitivity MRM mode | ESI+, Reserpine 1 pg on column, MRM609/195，S/N > 200,000 |
| Repeatability | ESI+, Tacrolimus 5pg on column with 10 injections, Peak area RSD < 1.5%, Retention time RSD<0.25 |
| Scan types | Full scan MS and selected ion for both Q1 and Q3, product ion scan, precursor ion scan, neutral loss or gain scan, Multiple reaction monitoring (MRM) |
| Dynamic range | 6 orders of magnitude |
| Ionization source | Ion Source housing with ESI Probe or APCI probe (max temp: 750ºC) ESI flow rate range: 5 μL/min to 3 mL/min APCI flow rate range: 200 µL/min to 3 mL/min |
| Software | B&C ITECH Chemstation V1.0 |
| Instrument Specification-Liquid Chromatograph (UHPLC) | |
| Flow rate range | 0.001 - 2.00 ml/min, 0.001 ml/min increments |
| Pressure range | 0-1300 bar |
| Flow precision | ≤ 0.075 % RSD or 0.005 min SD, whichever is greater, H2O in a flow range of 0.200 - 2.000 mL/min |
| Flow accuracy | ± 1% or ± 10 μL/min, whichever is greater, H2O in a flow range of 0.200 - 2.000 mL/min |
| Gradient composition range | 0 - 99% (A in B) |
| Gradient composition accuracy | ± 0.5 % absolute from 5 - 95%, H2O in a flow range of 0.200 - 2.000 mL/min |
| Gradient composition precision | ≤ 0.15% or 0.01 min SD, whichever is greater, H2O in a flow range of 0.200 - 2.000 mL/min |
| Injection modes | Full loop, partial loopfill and µL pickup mode |
| Injection volume | Programmable from 0 uL-100 uL,1 µL increments |
| Reproducibility | RSD £ 0.3% for full loop injections |
| RSD £ 0.5% for partial loopfill injections, injection volumes > 5 µL at constant pressure RSD £ 1.0% for µL pickup injections, injection volumes > 5 µL | |
| Carry-over | < 0.05% with programmable needle wash |
| Viscosity range | 0.1 - 5 cP |
| Sample tray cooling | Built-in Peltier cooling Range: 4°C to Ambient - 3°C Temp: air temperature in sample compartment: 4°C ± 2°C (at temperature sensor) (Temperature at relative humidity of 80% and ambient temperature of 25°C) |
| Needle wash | Inside and outside needle wash with drying. Wash can be programmed between injections and between vials/wells. |
| Sample capacity | Microtiter plates: 2 Vials: 2x 48 (1.5 mL) – optional Microtiter plates according to SBS standards. 96-well high and low and 384-well. |
| Column Oven Temperature control mode | air circulation with heating module |
| Temperature range | ambient+5°C - 60°C, with 1°C increments |
| Temperature stability | Better than 0.1 °C |
| Column capacity | Maximum 2 column, Length150 mm |
